Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet

H. Y. Koo; J. H. Kim; S. K. Hong; Y. N. Ko; H. C. Jang; D. S. Jung; J. M. Han; Y. J. Hong; Y. C. Kang; S. H. Kang; S. B. Cho

doi:10.1007/s12540-012-3010-6

Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet

H. Y. Koo
, J. H. Kim
, S. K. Hong
, Y. N. Ko
, H. C. Jang
, D. S. Jung
, J. M. Han
, Y. J. Hong
, Y. C. Kang^*
, S. H. Kang
, S. B. Cho

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

Fe powders as the heat pellet material for thermal batteries are prepared from iron oxide powders obtained by spray pyrolysis from a spray solution of iron nitrate with ethylene glycol. The iron oxide powders with hollow and thin wall structure produce Fe powders with elongated structure and fine primary particle size at a low reducing temperature of 615 °C. The mean size of the primary Fe powders with elongated structure decreases with increasing concentration of ethylene glycol dissolved into the spray solution. The heat pellets prepared from the fine-size Fe powders with elongated structure have good ignition sensitivities below 1 watt. The heat pellets formed from the Fe powders obtained from the spray solution with 0.5 M EG have an extremely high burn rate of 26 cms^-1.

Original language	English
Pages (from-to)	445-449
Number of pages	5
Journal	Metals and Materials International
Volume	18
Issue number	3
DOIs	https://doi.org/10.1007/s12540-012-3010-6
Publication status	Published - 2012 Jun
Externally published	Yes

Bibliographical note

Funding Information:
This work was supported by the Defense Acquisition Program Administration and the Agency for Defense Development under the contract UD070021AD.

Keywords

Chemical synthesis
Energy storage materials
Microstructure
Scanning electron microscopy (SEM)
Thermal battery

ASJC Scopus subject areas

Condensed Matter Physics
Mechanics of Materials
Metals and Alloys
Materials Chemistry

Access to Document

10.1007/s12540-012-3010-6

Cite this

Koo, H. Y., Kim, J. H., Hong, S. K., Ko, Y. N., Jang, H. C., Jung, D. S., Han, J. M., Hong, Y. J., Kang, Y. C., Kang, S. H., & Cho, S. B. (2012). Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet. Metals and Materials International, 18(3), 445-449. https://doi.org/10.1007/s12540-012-3010-6

@article{9ff32e56844c46dbbb634f86315d6eb5,

title = "Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet",

abstract = "Fe powders as the heat pellet material for thermal batteries are prepared from iron oxide powders obtained by spray pyrolysis from a spray solution of iron nitrate with ethylene glycol. The iron oxide powders with hollow and thin wall structure produce Fe powders with elongated structure and fine primary particle size at a low reducing temperature of 615 °C. The mean size of the primary Fe powders with elongated structure decreases with increasing concentration of ethylene glycol dissolved into the spray solution. The heat pellets prepared from the fine-size Fe powders with elongated structure have good ignition sensitivities below 1 watt. The heat pellets formed from the Fe powders obtained from the spray solution with 0.5 M EG have an extremely high burn rate of 26 cms-1.",

keywords = "Chemical synthesis, Energy storage materials, Microstructure, Scanning electron microscopy (SEM), Thermal battery",

author = "Koo, \{H. Y.\} and Kim, \{J. H.\} and Hong, \{S. K.\} and Ko, \{Y. N.\} and Jang, \{H. C.\} and Jung, \{D. S.\} and Han, \{J. M.\} and Hong, \{Y. J.\} and Kang, \{Y. C.\} and Kang, \{S. H.\} and Cho, \{S. B.\}",

note = "Funding Information: This work was supported by the Defense Acquisition Program Administration and the Agency for Defense Development under the contract UD070021AD.",

year = "2012",

month = jun,

doi = "10.1007/s12540-012-3010-6",

language = "English",

volume = "18",

pages = "445--449",

journal = "Metals and Materials International",

issn = "1598-9623",

publisher = "Korean Institute of Metals and Materials",

number = "3",

}

TY - JOUR

T1 - Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet

AU - Koo, H. Y.

AU - Kim, J. H.

AU - Hong, S. K.

AU - Ko, Y. N.

AU - Jang, H. C.

AU - Jung, D. S.

AU - Han, J. M.

AU - Hong, Y. J.

AU - Kang, Y. C.

AU - Kang, S. H.

AU - Cho, S. B.

N1 - Funding Information: This work was supported by the Defense Acquisition Program Administration and the Agency for Defense Development under the contract UD070021AD.

PY - 2012/6

Y1 - 2012/6

N2 - Fe powders as the heat pellet material for thermal batteries are prepared from iron oxide powders obtained by spray pyrolysis from a spray solution of iron nitrate with ethylene glycol. The iron oxide powders with hollow and thin wall structure produce Fe powders with elongated structure and fine primary particle size at a low reducing temperature of 615 °C. The mean size of the primary Fe powders with elongated structure decreases with increasing concentration of ethylene glycol dissolved into the spray solution. The heat pellets prepared from the fine-size Fe powders with elongated structure have good ignition sensitivities below 1 watt. The heat pellets formed from the Fe powders obtained from the spray solution with 0.5 M EG have an extremely high burn rate of 26 cms-1.

AB - Fe powders as the heat pellet material for thermal batteries are prepared from iron oxide powders obtained by spray pyrolysis from a spray solution of iron nitrate with ethylene glycol. The iron oxide powders with hollow and thin wall structure produce Fe powders with elongated structure and fine primary particle size at a low reducing temperature of 615 °C. The mean size of the primary Fe powders with elongated structure decreases with increasing concentration of ethylene glycol dissolved into the spray solution. The heat pellets prepared from the fine-size Fe powders with elongated structure have good ignition sensitivities below 1 watt. The heat pellets formed from the Fe powders obtained from the spray solution with 0.5 M EG have an extremely high burn rate of 26 cms-1.

KW - Chemical synthesis

KW - Energy storage materials

KW - Microstructure

KW - Scanning electron microscopy (SEM)

KW - Thermal battery

UR - https://www.scopus.com/pages/publications/84863816022

U2 - 10.1007/s12540-012-3010-6

DO - 10.1007/s12540-012-3010-6

M3 - Article

AN - SCOPUS:84863816022

SN - 1598-9623

VL - 18

SP - 445

EP - 449

JO - Metals and Materials International

JF - Metals and Materials International

IS - 3

ER -

Characteristics of fe powders prepared by spray pyrolysis from a spray solution with ethylene glycol as the source material of heat pellet

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this