Conformational study of a rigid-structured octathiabiscavitand from [2 + 2] coupling of caps and bridging units

Lee Jungbai; Kihang Choi; Kyungsoo Pack

doi:10.1016/s0040-4039(97)10195-2

Conformational study of a rigid-structured octathiabiscavitand from [2 + 2] coupling of caps and bridging units

Lee Jungbai, Kihang Choi, Kyungsoo Pack

Research output: Contribution to journal › Article › peer-review

9 Citations (Scopus)

Abstract

An octathiacavitand was stereoselectively obtained in good yield by [2 + 2] coupling reaction between a tetrakis(thiomethyl)cavitand and 1,2,4,5- tetrakis(bromomethyl)benzene. Its NOESY spectrum showed that its cavity was divided into two small ones by π - π stacking of two bridging benzene units.

Original language	English
Pages (from-to)	8203-8206
Number of pages	4
Journal	Tetrahedron Letters
Volume	38
Issue number	47
DOIs	https://doi.org/10.1016/s0040-4039(97)10195-2
Publication status	Published - 1997 Nov 24
Externally published	Yes

ASJC Scopus subject areas

Biochemistry
Drug Discovery
Organic Chemistry

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abstract = "An octathiacavitand was stereoselectively obtained in good yield by [2 + 2] coupling reaction between a tetrakis(thiomethyl)cavitand and 1,2,4,5- tetrakis(bromomethyl)benzene. Its NOESY spectrum showed that its cavity was divided into two small ones by π - π stacking of two bridging benzene units.",

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AU - Pack, Kyungsoo

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AB - An octathiacavitand was stereoselectively obtained in good yield by [2 + 2] coupling reaction between a tetrakis(thiomethyl)cavitand and 1,2,4,5- tetrakis(bromomethyl)benzene. Its NOESY spectrum showed that its cavity was divided into two small ones by π - π stacking of two bridging benzene units.

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Conformational study of a rigid-structured octathiabiscavitand from [2 + 2] coupling of caps and bridging units

Abstract

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