Formation of submicron copper sulfide particles using spray pyrolysis method

I. Wuled Lenggoro; Yun Chan Kang; Takafumi Komiya; Kikuo Okuyama; Noboru Tohge

doi:10.1143/jjap.37.l288

Formation of submicron copper sulfide particles using spray pyrolysis method

I. Wuled Lenggoro, Yun Chan Kang, Takafumi Komiya, Kikuo Okuyama, Noboru Tohge

Research output: Contribution to journal › Article › peer-review

22 Citations (Scopus)

Abstract

The morphology and crystalline phase of submicron copper sulfide particles prepared by spray pyrolysis method have been studied. In a nitrogen gas atmosphere, the covellite phase (CuS) spherical particles could be prepared using the solution with molar ratio of copper nitrate to thiourea and furnace temperatures of 1:2 at 200-300 °C, as well as of 1:5 at 200-600 °C. The crystalline phase of particles was highly depended on the composition of the precursors and the pyrolysis temperature. The sphericity of particles could be enhanced by increasing the temperature and prolonging the residence time of the droplets or particles in the furnace.

Original language	English
Pages (from-to)	L288-L290
Journal	Japanese Journal of Applied Physics, Part 2: Letters
Volume	37
Issue number	3 A
DOIs	https://doi.org/10.1143/jjap.37.l288
Publication status	Published - 1998
Externally published	Yes

ASJC Scopus subject areas

Engineering(all)
Physics and Astronomy(all)

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abstract = "The morphology and crystalline phase of submicron copper sulfide particles prepared by spray pyrolysis method have been studied. In a nitrogen gas atmosphere, the covellite phase (CuS) spherical particles could be prepared using the solution with molar ratio of copper nitrate to thiourea and furnace temperatures of 1:2 at 200-300 °C, as well as of 1:5 at 200-600 °C. The crystalline phase of particles was highly depended on the composition of the precursors and the pyrolysis temperature. The sphericity of particles could be enhanced by increasing the temperature and prolonging the residence time of the droplets or particles in the furnace.",

author = "Lenggoro, {I. Wuled} and Kang, {Yun Chan} and Takafumi Komiya and Kikuo Okuyama and Noboru Tohge",

year = "1998",

doi = "10.1143/jjap.37.l288",

language = "English",

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T1 - Formation of submicron copper sulfide particles using spray pyrolysis method

AU - Lenggoro, I. Wuled

AU - Kang, Yun Chan

AU - Komiya, Takafumi

AU - Okuyama, Kikuo

AU - Tohge, Noboru

PY - 1998

Y1 - 1998

N2 - The morphology and crystalline phase of submicron copper sulfide particles prepared by spray pyrolysis method have been studied. In a nitrogen gas atmosphere, the covellite phase (CuS) spherical particles could be prepared using the solution with molar ratio of copper nitrate to thiourea and furnace temperatures of 1:2 at 200-300 °C, as well as of 1:5 at 200-600 °C. The crystalline phase of particles was highly depended on the composition of the precursors and the pyrolysis temperature. The sphericity of particles could be enhanced by increasing the temperature and prolonging the residence time of the droplets or particles in the furnace.

AB - The morphology and crystalline phase of submicron copper sulfide particles prepared by spray pyrolysis method have been studied. In a nitrogen gas atmosphere, the covellite phase (CuS) spherical particles could be prepared using the solution with molar ratio of copper nitrate to thiourea and furnace temperatures of 1:2 at 200-300 °C, as well as of 1:5 at 200-600 °C. The crystalline phase of particles was highly depended on the composition of the precursors and the pyrolysis temperature. The sphericity of particles could be enhanced by increasing the temperature and prolonging the residence time of the droplets or particles in the furnace.

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DO - 10.1143/jjap.37.l288

M3 - Article

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SN - 0021-4922

VL - 37

SP - L288-L290

JO - Japanese Journal of Applied Physics, Part 1: Regular Papers & Short Notes

JF - Japanese Journal of Applied Physics, Part 1: Regular Papers & Short Notes

IS - 3 A

ER -

Formation of submicron copper sulfide particles using spray pyrolysis method

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