Abstract
A two-stage continuous microreactor system was use to synthesize the materials for an organic light emitting diode. The split and recombine type of micromixers were suitable for the two-stage reaction including lithium-bromo exchange reaction. The two-stage synthesis was carried out under non-cryogenic conditions by taking full advantage of microstructured reaction systems. In a first stage, the unstable intermediate, naphthyl lithium was synthesized with maximum yield and consumed immediately in the second stage micromixer. The naphthyl-substituted anthracene was obtained with 97% purity.
Original language | English |
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Pages (from-to) | S17-S20 |
Journal | Chemical Engineering Journal |
Volume | 135 |
Issue number | SUPPL. 1 |
DOIs | |
Publication status | Published - 2008 Jan 15 |
Bibliographical note
Funding Information:This work has been supported by the Next Generation Novel Technology Development Program of the Ministry of Commerce, Industry and Energy (MOCIE) under the project title of “Development of Micro-Optical and Thermofluidic Devices with High Functionality.”
Keywords
- Bromonaphthalene
- Electron transport layer
- Microreaction technology
ASJC Scopus subject areas
- General Chemistry
- Environmental Chemistry
- General Chemical Engineering
- Industrial and Manufacturing Engineering