Synthesis and characterization of nanocrystalline mercury telluride by sonochemical method

H. Song; K. Cho; H. Kim; J. S. Lee; B. Min; H. S. Kim; S. W. Kim; T. Noh; S. Kim

doi:10.1016/j.jcrysgro.2004.05.112

Synthesis and characterization of nanocrystalline mercury telluride by sonochemical method

H. Song, K. Cho, H. Kim, J. S. Lee, B. Min, H. S. Kim, S. W. Kim, T. Noh, S. Kim

Research output: Contribution to journal › Article › peer-review

28 Citations (Scopus)

Abstract

Mercury telluride (HgTe) nanorods and nanoparticles were synthesized at room temperature via sonochemical method. The crystalline HgTe nanorods were formed from mercury perchlorate hydrate and tellurium powder in an ethylenediamine solvent system mixed with a complexing agent of 1-thioglycerol. In addition, the HgTe nanoparticles and the amorphous Te material were produced in the same solvent system without the 1-thioglycerol. The synthesized HgTe nanorods, HgTe nanoparticles, and amorphous Te were characterized by X-ray diffraction, Raman spectroscopy, transmission electron microscopy, and high-resolution transmission electron microscopy. In addition, the role of 1-thioglycerol in the synthesis of the nanocrystalline HgTe is discussed in this paper.

Original language	English
Pages (from-to)	317-323
Number of pages	7
Journal	Journal of Crystal Growth
Volume	269
Issue number	2-4
DOIs	https://doi.org/10.1016/j.jcrysgro.2004.05.112
Publication status	Published - 2004 Sept 1

Bibliographical note

Funding Information:
This work was supported by the Korean Ministry of Science and Technology as a part of the ‘04 Nuclear R&D Program, Grant No. M2-0363-00-0052, Grant No. R01-1999-000-00230-0, Grant No. R01-2002-000-00504-0 from the Basic Research Program of the Korea Science & Engineering Foundation, and National R&D project for Nano Science and Technology.

Keywords

A1. Complexing agent
A1. Sonochemistry
B1. Mercury telluride
B1. Nanoparticles

ASJC Scopus subject areas

Condensed Matter Physics
Inorganic Chemistry
Materials Chemistry

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10.1016/j.jcrysgro.2004.05.112

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title = "Synthesis and characterization of nanocrystalline mercury telluride by sonochemical method",

abstract = "Mercury telluride (HgTe) nanorods and nanoparticles were synthesized at room temperature via sonochemical method. The crystalline HgTe nanorods were formed from mercury perchlorate hydrate and tellurium powder in an ethylenediamine solvent system mixed with a complexing agent of 1-thioglycerol. In addition, the HgTe nanoparticles and the amorphous Te material were produced in the same solvent system without the 1-thioglycerol. The synthesized HgTe nanorods, HgTe nanoparticles, and amorphous Te were characterized by X-ray diffraction, Raman spectroscopy, transmission electron microscopy, and high-resolution transmission electron microscopy. In addition, the role of 1-thioglycerol in the synthesis of the nanocrystalline HgTe is discussed in this paper.",

keywords = "A1. Complexing agent, A1. Sonochemistry, B1. Mercury telluride, B1. Nanoparticles",

author = "H. Song and K. Cho and H. Kim and Lee, {J. S.} and B. Min and Kim, {H. S.} and Kim, {S. W.} and T. Noh and S. Kim",

note = "Funding Information: This work was supported by the Korean Ministry of Science and Technology as a part of the {\textquoteleft}04 Nuclear R&D Program, Grant No. M2-0363-00-0052, Grant No. R01-1999-000-00230-0, Grant No. R01-2002-000-00504-0 from the Basic Research Program of the Korea Science & Engineering Foundation, and National R&D project for Nano Science and Technology.",

year = "2004",

month = sep,

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doi = "10.1016/j.jcrysgro.2004.05.112",

language = "English",

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pages = "317--323",

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TY - JOUR

T1 - Synthesis and characterization of nanocrystalline mercury telluride by sonochemical method

AU - Song, H.

AU - Cho, K.

AU - Kim, H.

AU - Lee, J. S.

AU - Min, B.

AU - Kim, H. S.

AU - Kim, S. W.

AU - Noh, T.

AU - Kim, S.

N1 - Funding Information: This work was supported by the Korean Ministry of Science and Technology as a part of the ‘04 Nuclear R&D Program, Grant No. M2-0363-00-0052, Grant No. R01-1999-000-00230-0, Grant No. R01-2002-000-00504-0 from the Basic Research Program of the Korea Science & Engineering Foundation, and National R&D project for Nano Science and Technology.

PY - 2004/9/1

Y1 - 2004/9/1

N2 - Mercury telluride (HgTe) nanorods and nanoparticles were synthesized at room temperature via sonochemical method. The crystalline HgTe nanorods were formed from mercury perchlorate hydrate and tellurium powder in an ethylenediamine solvent system mixed with a complexing agent of 1-thioglycerol. In addition, the HgTe nanoparticles and the amorphous Te material were produced in the same solvent system without the 1-thioglycerol. The synthesized HgTe nanorods, HgTe nanoparticles, and amorphous Te were characterized by X-ray diffraction, Raman spectroscopy, transmission electron microscopy, and high-resolution transmission electron microscopy. In addition, the role of 1-thioglycerol in the synthesis of the nanocrystalline HgTe is discussed in this paper.

AB - Mercury telluride (HgTe) nanorods and nanoparticles were synthesized at room temperature via sonochemical method. The crystalline HgTe nanorods were formed from mercury perchlorate hydrate and tellurium powder in an ethylenediamine solvent system mixed with a complexing agent of 1-thioglycerol. In addition, the HgTe nanoparticles and the amorphous Te material were produced in the same solvent system without the 1-thioglycerol. The synthesized HgTe nanorods, HgTe nanoparticles, and amorphous Te were characterized by X-ray diffraction, Raman spectroscopy, transmission electron microscopy, and high-resolution transmission electron microscopy. In addition, the role of 1-thioglycerol in the synthesis of the nanocrystalline HgTe is discussed in this paper.

KW - A1. Complexing agent

KW - A1. Sonochemistry

KW - B1. Mercury telluride

KW - B1. Nanoparticles

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M3 - Article

AN - SCOPUS:4344620936

SN - 0022-0248

VL - 269

SP - 317

EP - 323

JO - Journal of Crystal Growth

JF - Journal of Crystal Growth

IS - 2-4

ER -

Synthesis and characterization of nanocrystalline mercury telluride by sonochemical method

Abstract

Bibliographical note

Keywords

ASJC Scopus subject areas

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