The aualsis of dioxin-like pcbs in fishes and shelifishes using accelerated solvent extraction (ASE) system and multilayer column chromatography

Jung Hyuck Suh; Keum Soon Oh; Seongssoo Park; So Young Chung; You Sub Sho; Jung Soo Kim; Seoung Chul Jung; Jong Ok Lee; Hee Yun Kim; Gun Jo Woo

The aualsis of dioxin-like pcbs in fishes and shelifishes using accelerated solvent extraction (ASE) system and multilayer column chromatography

Jung Hyuck Suh, Keum Soon Oh, Seongssoo Park, So Young Chung, You Sub Sho, Jung Soo Kim, Seoung Chul Jung, Jong Ok Lee, Hee Yun Kim, Gun Jo Woo

Department of Biotechnology

Research output: Contribution to journal › Article › peer-review

Abstract

In this, study, an analytical method was optimized for detecting dioxin-like PCBs in fish and shellfish. Hera, homogenized samples were extracted using an accelerated solvent extraction (ASE) system with 33 mL ceel sixe. Multilayer column choromatography, which consisted of actidic, basic, and neutral silica gels, was used for the clen up of the extracts. The instrumental analysis was executed by HRGC/HRMS to a resolution od 10,000 using 4 window multiple ion detection (MID) mode. For the results, the average recoveries ranged from 94.1 to 104.1% (±8.4) and the limit of detection was approximately 0.1 pg/g at S/N ratio >3. Finally, the detected concentration of dioxi-like PCBs for fish shellfish were in the rang of 0.030-1.836 pg TEQ/g.

Original language	English
Pages (from-to)	122-127
Number of pages	6
Journal	Korean Journal of Food Science and Technology
Volume	39
Issue number	2
Publication status	Published - 2007

Keywords

Accelrated solvent extraction
Dioxin-like PCBs
Fishes and shellfishes
Food

ASJC Scopus subject areas

Biotechnology
Food Science
Applied Microbiology and Biotechnology

Cite this

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title = "The aualsis of dioxin-like pcbs in fishes and shelifishes using accelerated solvent extraction (ASE) system and multilayer column chromatography",

abstract = "In this, study, an analytical method was optimized for detecting dioxin-like PCBs in fish and shellfish. Hera, homogenized samples were extracted using an accelerated solvent extraction (ASE) system with 33 mL ceel sixe. Multilayer column choromatography, which consisted of actidic, basic, and neutral silica gels, was used for the clen up of the extracts. The instrumental analysis was executed by HRGC/HRMS to a resolution od 10,000 using 4 window multiple ion detection (MID) mode. For the results, the average recoveries ranged from 94.1 to 104.1% (±8.4) and the limit of detection was approximately 0.1 pg/g at S/N ratio >3. Finally, the detected concentration of dioxi-like PCBs for fish shellfish were in the rang of 0.030-1.836 pg TEQ/g.",

keywords = "Accelrated solvent extraction, Dioxin-like PCBs, Fishes and shellfishes, Food",

author = "Suh, {Jung Hyuck} and Oh, {Keum Soon} and Seongssoo Park and Chung, {So Young} and Sho, {You Sub} and Kim, {Jung Soo} and Jung, {Seoung Chul} and Lee, {Jong Ok} and Kim, {Hee Yun} and Woo, {Gun Jo}",

year = "2007",

language = "English",

volume = "39",

pages = "122--127",

journal = "Korean Journal of Food Science and Technology",

issn = "0367-6293",

publisher = "Tong Kwahak Hoe",

number = "2",

}

TY - JOUR

T1 - The aualsis of dioxin-like pcbs in fishes and shelifishes using accelerated solvent extraction (ASE) system and multilayer column chromatography

AU - Suh, Jung Hyuck

AU - Oh, Keum Soon

AU - Park, Seongssoo

AU - Chung, So Young

AU - Sho, You Sub

AU - Kim, Jung Soo

AU - Jung, Seoung Chul

AU - Lee, Jong Ok

AU - Kim, Hee Yun

AU - Woo, Gun Jo

PY - 2007

Y1 - 2007

N2 - In this, study, an analytical method was optimized for detecting dioxin-like PCBs in fish and shellfish. Hera, homogenized samples were extracted using an accelerated solvent extraction (ASE) system with 33 mL ceel sixe. Multilayer column choromatography, which consisted of actidic, basic, and neutral silica gels, was used for the clen up of the extracts. The instrumental analysis was executed by HRGC/HRMS to a resolution od 10,000 using 4 window multiple ion detection (MID) mode. For the results, the average recoveries ranged from 94.1 to 104.1% (±8.4) and the limit of detection was approximately 0.1 pg/g at S/N ratio >3. Finally, the detected concentration of dioxi-like PCBs for fish shellfish were in the rang of 0.030-1.836 pg TEQ/g.

AB - In this, study, an analytical method was optimized for detecting dioxin-like PCBs in fish and shellfish. Hera, homogenized samples were extracted using an accelerated solvent extraction (ASE) system with 33 mL ceel sixe. Multilayer column choromatography, which consisted of actidic, basic, and neutral silica gels, was used for the clen up of the extracts. The instrumental analysis was executed by HRGC/HRMS to a resolution od 10,000 using 4 window multiple ion detection (MID) mode. For the results, the average recoveries ranged from 94.1 to 104.1% (±8.4) and the limit of detection was approximately 0.1 pg/g at S/N ratio >3. Finally, the detected concentration of dioxi-like PCBs for fish shellfish were in the rang of 0.030-1.836 pg TEQ/g.

KW - Accelrated solvent extraction

KW - Dioxin-like PCBs

KW - Fishes and shellfishes

KW - Food

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SN - 0367-6293

VL - 39

SP - 122

EP - 127

JO - Korean Journal of Food Science and Technology

JF - Korean Journal of Food Science and Technology

IS - 2

ER -

The aualsis of dioxin-like pcbs in fishes and shelifishes using accelerated solvent extraction (ASE) system and multilayer column chromatography

Abstract

Keywords

ASJC Scopus subject areas

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